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2019/4/2 · Headspace sampling refers to the gas space in a chromatography vial containing a liquid sample. The liquid sample is a solvent, containing material to be analysed. E.g. volatile organic compounds in environmental samples, alcohols in blood, residual solvents in pharmaceutical products, plastics, flavour compounds in beverages and food, coffee, fragrances in perfumes and cosmetics.
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Automating the liquid-liquid extraction workflow minimizes cost and effort by reducing sample and solvent consumption. Combining automated in-vial LLE with large-volume injection and a highly sensitive GC-MS/MS system enables the detection of different classes of contaminants at ultra-low levels on a single analytical system.
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2015/9/15 · This work reports on a full evaporation headspace gas chromatographic (FE HS-GC) method for simultaneously determining the ethanol (EtOH) and methanol (MeOH) content in wines. A small sample (10 μL) was placed in a headspace sample vial, and a near-complete mass transfer of ethanol and methanol from the liquid sample to the vapor phase was obtained within three minutes at a
urine sample with extrelute NT3 using GCMS. The synthetic cannabinoids could be detected as parent compound with no metabolites was identified. In the recent report, we developed a liquid chromatography–high resolution mass spectrometry (LC-HRMSthe 5F
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Due to the simplicity of application and the possibility of automation, sample filtration is well suited for a clinical and forensic laboratory. To monitor alcohol consumption, an analytical method based on liquid chromatography-tandem mass spectrometry (LC-MS/MS
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