2019/7/10 · HPLC analysis was conducted in 0.1 M TEAA, pH 9.70 ± 0.05 (triethylammonium acetate) buffer with 5% acetonitrile (ACN) and 30% ACN as the two mobile phases. 0.1 M TEAA buffer was prepared by adding 5.6 mL of glacier acetic acid to 950 mL of deionized