The sample was then divided into two parts, and each part was sealed in a 50-mL crimp-top vial with a PTFE silicone-lined cap. One vial was exposed to light from a 100-W tungsten bulb (6000 lux
VOCs HS-SPME DVB/CAR/PDMS GC-FID 0.02 and 490 ng g À1 [71] Soil and sand PAHs Cold fiber HS-SPME PDMS GC-FID Not reported [72] Soil Nitro explosive compounds SPME Carbon ceramic copper
1/4/2006 · All samples, standards and blanks were prepared in 6-mL glass crimp top vials sealed with aluminum seal/PTFE/silicon septum tops. One milliliter of fluorobenzene surrogate spike solution (4 mg/L), 1.000 g NaCl, and a small stir bar to agitate the solution were added to each sample and standard vial before sealing.
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methane layer was removed to a crimp-top GC vial for analysis. The GC − MS analysis was performed using an Aijiren C GC/ MS. A 1 μ L aliquot of each sample was injected onto a 30 m
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Academia.edu is a platform for academics to share research papers. Microbial diversity and molecular signals controlling plant-microbe interaction in the rhizosphere of grasses
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Sealed crimp‐top vials (27 ml) were sparged for 5 min with nitrogen, and 9 ml of the cell suspension and 1 ml of 1 M formate were added to the bottles which were incubated at 37 C with shaking for 1 h.
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Adults were briefly anesthesized with CO2 and placed in a glass GC vial with a teflon-lined crimp top. The septum was pierced, and then 150 ml of hexane was injected and allowed to soak the insect for 1 min, after which the hexane was removed with a syringe and placed in a tared foil planchet.