Concentration in the mVAP can be combined with a wide variety of sample preparation and clean-up techniques such as SPE, dispersive SPE (DPX), liquid/liquid extraction or filtration with the significant benefit of automated injection of the concentrated sample into a GC/MS or LC/MS system.
Oct 23, 2019 · After centrifugation 80 μl of the organic phase containing the products were transferred to a 1.5 ml GC vial with a small insert (200 μl). Samples were measured in GC‐FID. 2.3.4 Product identification by GC–MS
Gas Chromatography-Mass Spectrometry (GC-MS) Analysis The GC-MS was carried out using total ion monitoring mode on a Varian 3800 gas chromatograph interfaced to a Varian Saturn ion trap 2200 GC-MS spectrometer. The temperatures of transfer line and ion source were 280°C and 275°C respectively. Ions were obtained by electron ionization mode.
Finally the juice filled by a seal dark glass vial and and kept frozen at18 °C upon analysis[21]. 2.1 Gas Chromatography-Mass Spectrometry (GC-MS) Analysis The component identification of methanolic extract of pomegranate juice (Salami variety) was done using Shimadzu GC-2010 gas chromatography coupled with QP2010 mass spectrometer.
Gas chromatography–Mass Spectrometry (GC–MS): For GC-MS analysis, the sample was injected into a HP-5 column (30 m X 0.25 mm i.d. with 0.25 μm film thickness, Aijiren technologies N JEOL GC Mate II GC-MS model). Following chromatographic conditions were used: Helium as carrier gas, flow rate of 1 mL/min and the injector
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Aijiren headspace vials are offered as 10 mL vial and 20 mL certified screw vials and certified crimp vials, clear glass or amber glass headspace vials and associated 11 mm crimp caps , 18 mm screw caps, 20 mm crimp caps and 22 mm crimp caps while being are engineered to prevent sample contamination providing a consistent, secure seal of the .
simultaneously using the GC-FID.8 With the success of these methods using the FID, capillary gas chromatography-mass spectroscopy (GC-MS) seemed an ideal approach. Although the MS detector is more expensive, the GC-MS combines all the positive aspects of this methodology and promises very accurate results using a variety of source matrices and
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11.1.2.6 Collect supernatant and transfer 1 mL into a GC vial for instrumental analysis. 11.1.2.7 Add 50 µL sorbitol solution (protectant) and 20 µL 5000 ng/mL injection standard (BFB) to the GC vials prior to injection. 11.2 GC-MS/MS Analysis Sample measurements were carried out using the TRACE 1310 gas chromatograph coupled to the TSQ